Initial Characterisation of SK01 Sanidine: A Candidate 40Ar/39Ar Reference Material     

Youjuan Li  Brian R. Jicha  Wanfeng Zhang  Wen Chen  Brad S. Singer  Dewen Zheng  Huaiyu He 《Geostandards and Geoanalytical Research》2023,47(3):657-668

The precision and accuracy of ⁴⁰Ar/³⁹Ar dates are ultimately linked to co-irradiated reference materials of known age. Here we provide new data from the SK01 sanidine, which was analysed in three different laboratories to evaluate it as a ⁴⁰Ar/³⁹Ar reference material. Aliquots of 5 mg, incrementally heated in two laboratories, yielded indistinguishable results with a weighted mean age of 27.58 ± 0.06 Ma (95% confidence level). Single-crystal step heating and single-crystal total fusion analyses of SK01 sanidine were undertaken in the third laboratory to further test the intracrystalline homogeneity. For the seven step-heating analyses, six crystals yielded nearly concordant age spectra with ⁴⁰Ar/³⁹Ar ages ranging from 26.853 ± 0.094 Ma to 26.963 ± 0.067 Ma, whereas one crystal gave an older age of 27.774 ± 0.071 Ma with a slightly discordant age spectrum. Twenty-three single-crystal total fusion analyses yielded ⁴⁰Ar/³⁹Ar ages ranging from 27.070 ± 0.108 Ma to 27.736 ± 0.062 Ma with a dispersion of ~ 3.8%. The older ages from single-crystal total fusion dates are interpreted to reflect an inherited or excess argon component in some crystals. This is an initial characterisation of the SK01 sanidine, and additional work needs to be conducted to further evaluate the age dispersion so that it can be utilised as a ⁴⁰Ar/³⁹Ar reference material.  相似文献   

东北三省城乡协调发展格局及影响因素   总被引：3，自引：2，他引：1  

黄禹铭 《地理科学》2019,39(8):1302-1311

以东北三省36个地区为研究对象,系统构建了城乡协调的指标体系,采用基尼系数、空间自相关和空间回归等方法探讨了2005年、2010年和2015年东北三省城乡协调的空间格局和影响机制。研究表明:① 东北三省城乡协调度的区域差异不断扩大且具有明显的空间集聚特征,但集聚程度趋于减弱。② 不同地区城乡协调水平变化各异。研究期内,大连市和锦州市一直处于高水平城乡协调状态,朝阳市长期处于低水平城乡协调状态。鹤岗市和七台河市城乡协调度位次上升最明显,哈尔滨市和辽源市城乡协调度位次下降最显著。③ 从空间格局来看,中级城乡协调区增多且向北移动,初级城乡协调区减少且向中部集中,“南北高,中间低”的城乡协调格局基本形成。与此同时,城乡协调的冷热点均不断收缩,空间极化效应趋于减弱。④ 城镇化和农业规模化经营是促进东北城乡协调发展的主要力量,工业化并未显著促进东北城乡协调发展且与城乡协调发展负相关,农业现代化经营对城乡协调发展有正向作用,交通因素在近些年的促进作用逐渐凸显,经济发展水平与信息化水平对东北城乡协调发展的作用还不明显。  相似文献   

轴压作用下双金属复合管组合作用与承载力分析     

朱振兴  杨璐  王法承  方成 《海洋工程》2019,37(4):98-106

为探究轴压作用下双金属复合海底管道的组合作用与承载性能,对双金属复合海底管道进行了试验研究和理论分析。开展了不锈钢衬管材料性能试验,对比了国际主流不锈钢本构关系模型和试验结果。利用ABAQUS建立了精细化的双金属复合管道轴压试验有限元模型,系统研究了关键参数如复合工艺产生的环向复合应力、钢管初始缺陷幅值等对双金属复合管在轴压作用下力学性能的影响规律。通过对比已有轴压双金属复合管道试验结果,验证有限元模型。基于验证的有限元模型,对轴压作用下双金属复合管道的组合作用以及径厚比和材料强度对承载力的影响进行了分析。结果表明双金属复合管道的轴压极限承载力主要取决于基管的截面屈服荷载,并随着管径和材料强度的提高而增大。并依据分析结果对双金属复合海底管道的设计提出建议。  相似文献   

Duluth Complex apatites: Age reference material for LA–ICP–MS‐based fission‐track dating     

Hideki Iwano  Tohru Danhara  Takashi Yuguchi  Takafumi Hirata  Masatsugu Ogasawara 《地学学报》2019,31(3):247-256

Anorthositic series apatites of the Duluth Complex, Minnesota, USA, have high spontaneous fission‐track densities of up to ~10⁷ cm^–2 and a homogeneous age of ~900 Ma, allowing high‐precision fission‐track dating based on LA–ICP–MS U analysis. Absolute fission‐track dating, track‐length measurement and chemical composition analysis were performed to evaluate a cooling history, which is essential for age reference materials. Preliminary inverse modelling for a sample with a shortened track‐length distribution yielded a monotonic cooling history from ~100°C at 925 Ma. The apatites incur an over‐etching problem when employing the commonly used etching protocol involving 5.5 M HNO₃.  相似文献   

深海滑坡灾害的物质点法模拟     

董友扣  马家杰  王栋  RANDOLPH Mark 《海洋工程》2019,37(5):141-147

深海滑坡可以沿着斜坡搬运大量沉积物,是危害巨大的海洋地质灾害之一。评估深海滑坡的流滑机制并量化分析其对海底结构物的冲击对海洋资源的开发利用至关重要。采用物质点法对滑坡的滑动特性进行了总应力分析。设计了三组不同的土体、海床参数,展现了三种不同的滑动形态:延展、块体和扩张。随后复现了流滑体对部分暴露管线的冲击过程,并对冲击力的稳定值进行了分析,分析中考虑了流滑体的惯性、抗剪强度和静压力的影响。研究表明,物质点法能够用于模拟深海滑坡的流滑过程及其对海底结构物的冲击,可以为海洋工程中的实际设计工作提供服务。  相似文献   

Modelling landslides in unsaturated slopes subjected to rainfall infiltration using material point method          下载免费PDF全文

Samila Bandara  Alessio Ferrari  Lyesse Laloui 《国际地质力学数值与分析法杂志》2016,40(9):1358-1380

This paper presents a dynamic fully coupled formulation for saturated and unsaturated soils that undergo large deformations based on material point method. Governing equations are applied to porous material while considering it as a continuum in which the pores of the solid skeleton are filled with water and air. The accuracy of the developed method is tested with available experimental and numerical results. The developed method has been applied to investigate the failure and post‐failure behaviour of rapid landslides in unsaturated slopes subjected to rainfall infiltration using two different bedrock geometries that lie below the top soil. The models show different failure and post‐failure mechanisms depending on the bedrock geometry and highlight the negative effects of continuous rain infiltrations. Copyright © 2016 John Wiley & Sons, Ltd.  相似文献   

Using archaeological data and sediment parameters to review the formation of the Gravettian layers at Krems-Wachtberg     

Marc Händel  Roswitha Thomas  Tobias Sprafke  Philipp Schulte  Michael Brandl  Ulrich Simon  Thomas Einwögerer 《第四纪科学杂志》2021,36(8):1397-1413

  相似文献   

双能CT成像基材料分解法的理论误差分析     

郑鹏  郝佳  邢宇翔 《CT理论与应用研究》2011,20(2):153-162

双能X射线计算机断层成像技术(DECT)能够准确地重建物质的有效原子序数和电子密度信息,是一种有效的物质辨别技术.基材料分解法是求解DECT重建问题的主要方法之一.但目前应用此方法得到的重建结果误差较大,并且对于金属伪影抑制能力也较差.本文分析了DECT基材料分解法重建结果的误差来源和形成机制,阐释了其对金属伪影抑制作...  相似文献   

Metamorphic history of the South Tibetan Detachment System,Mt. Everest region,revealed by RSCM thermometry and phase equilibria modelling   总被引：2，自引：0，他引：2  

J. M. COTTLE  D. J. WATERS  O. BEYSSAC  M. J. JESSUP 《Journal of Metamorphic Geology》2011,29(5):561-582

This study combines microstructural observations with Raman spectroscopy on carbonaceous material (RSCM), phase equilibria modelling and U–Pb dating of titanite to delineate the metamorphic history of a well‐exposed section through the South Tibetan Detachment System (STDS) in the Dzakaa Chu valley of Southern Tibet. In the hanging wall of the STDS, undeformed Tibetan Sedimentary Series rocks consistently record peak metamorphic temperatures of ～340 °C. Temperatures increase down‐section, reaching ～650 °C at the base of the shear zone, defining an apparent metamorphic field gradient of ～310 °C km^?1 across the entire structure. U–Th–Pb geochronological data indicate that metamorphism and deformation at high temperatures occurred over a protracted period from at least 20 to 13 Ma. Deformation within this 1‐km‐thick zone of distributed top‐down‐to‐the‐northeast ductile shear included a strong component of vertical shortening and was responsible for significant condensing of palaeo‐isotherms along the upper margin of the Greater Himalayan Series (GHS). We interpret the preservation of such a high metamorphic gradient to be the result of a progressive up‐section migration in the locus of deformation within the zone. This segment of the STDS provides a detailed thermal and kinematic record of the exhumation of footwall GHS rocks from beneath the southern margin of the Tibetan plateau.  相似文献   

铜镍硫化物铼-锇标准物质定值的溯源性讨论及总不确定度评估     

屈文俊  李超  杜安道 《岩矿测试》2011,30(6):664-668

对按国家一级标准物质技术规范研制的铜镍硫化物Re-Os标准物质定值的溯源性及其总不确定度进行讨论与评估。铜镍硫化物标准物质样品采用Carius管溶解,高精度的TRITON同位素质谱仪、MAT-262热电离质谱仪、四极杆等离子体质谱仪、多接收器等离子体质谱仪和高分辨四极杆等离子体质谱仪测量Re、Os含量和Os同位素比值,其中Re-Os含量可以溯源至基准物质,而187Os/188Os同位素比值可以溯源至国际纯粹与应用化学联合会(IUPAC)。在定值数据误差计算时,采用国际通用的ISOPLOT软件利用加权的方法对数据进行处理;在合成总不确定度时,考虑了物质的均匀性和稳定性,同时考虑了稀释剂标定和同位素丰度以及称量误差等影响测定因素的不确定度。标准值的不确定度由三部分组成:第一部分是通过所有参与定值数据,采用ISOPLOT软件,利用加权的方法对数据进行计算处理得到的不确定度;第二部分是物质的均匀性和稳定性的不确定度;第三部分是影响测定其他因素的不确定度。  相似文献